An initiator was intercalated into the interlayer spacings of montmorillonite clay, from which poly(styrene-block-butyl acrylate) silicate nanocomposites were prepared using atom transfer radical polymerization. A mixture of exfoliated structure and intercalated structure was produced in the nanocomposite. The poly(butyl acrylate) chains form microdomains with an average size of 2−5 nm.
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Zhao et al. (2003) studied this question.
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