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Areno‐anellated [3.3.n]propellanes with n = 2, 3, and 4 are easily accesible by palladium‐catalyzed domino coupling processes of the pentalene system 8 with various aryl iodides. The X‐ray structure investigations reveled a noteworthy elongation of the central CC single bond of these propellanes to ca. 162 pm.
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Dyker et al. (1997) studied this question.
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