The unnatural L‐1,1‐α‐disaccharides were synthesized from acylfurans using a palladium‐catalyzed glycosylation reaction. The 1,1‐α‐manno‐disaccharides were achieved in six total steps starting from an acylfuran. The overall efficiency of this protocol was the use of highly diastereoselective palladium‐catalyzed glycosylation, reduction, and dihydroxylation.
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Babu et al. (2005) studied this question.
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