Pure and doped nanocrystalline ZnO films of 0.1–1.0 μm thickness were prepared by spray pyrolysis techniques. Structural properties of these thin films were investigated by electron microscopy, force microscopy, x-ray diffractometry, ellipsometry, and optical spectroscopy. Using Ti:sapphire laser pulses, the second-harmonic efficiency of the films was measured. A correlation between measured efficiency and the grain shape in the polycrystalline layers is reported. Moreover, measurements of the angular dependence of the second-harmonic intensity are indicative of the dominant role of bulk effects over surface effects for the second-harmonic generation in such films.
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Neumann et al. (2004) studied this question.
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