By the example of multilayer MoS 2 nanotubes the capabilities of the X-ray diffraction method in determining possible polytypic forms of layered metal dichalcogenides, which may appear due to the nanostructuring of these compounds, are discussed. The conclusion about a low information value of the X-ray diffraction method is drawn, therefore the experimental analysis of the polytypic composition of nanostructures of metal dichalcogenides needs to attract electron microscopy and electronoй tomography methods.
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Enyashin et al. (2013) studied this question.
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