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A one‐pot facile synthesis of thiazole‐2(3H)‐thiones (4) has been achieved by hypervalent iodine oxidation of ketones (1) using [hydroxy(tosyloxy)iodo]benzene, followed by the treatment of the reaction mixture with dithiocarbamate salts (3). The intermediate α‐tosyloxyketones (2) have also been isolated and converted to the target compounds.
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Aggarwal et al. (2004) studied this question.
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