A highly ordered LiNi0.5Mn0.5O2 nanowire array was prepared using a porous anodic aluminium oxide (AAO) template from a sol–gel solution containing Li(OAc), Ni(OAc)2 and Mn(OAc)2. Electron microscopy results show that LiNi0.5Mn0.5O2 nanowires of uniform length and diameter are obtained, and that the length and diameter of the LiNi0.5Mn0.5O2 nanowires are dependent upon the pore diameter and the thickness of the applied AAO template. X-Ray diffraction and electron diffraction investigations demonstrate that the LiNi0.5Mn0.5O2 nanowires have a layered structure of LiNi0.5Mn0.5O2. X-ray photoelectron spectroscopy indicates that a nearly stoichiometric layered LiNi0.5Mn0.5O2 material has been obtained.
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Hu‐Lin Li (2002) studied this question.
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