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A new crystalline compound has been synthesized by trimethylsilylation of tetraethylammonium silicate which was identified by means of gas chromatography, mass spectrometry, 29Si NMR and X‐ray analysis to be a eage‐like double three‐ring silicic acid trimethylsilyl ester containing six inequivalent SiO4 tetrahedra and trimethylsilyl groups.
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Hoebbel et al. (1987) studied this question.
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