Minimum effort—maximum effect: Deoxygenated oligosaccharides and glycoconjugates are prepared in high yields with minimum purification from thioglycosides (see scheme) by exclusively employing reagents that are removed by simple filtration. New solid-phase-assisted synthetic protocols for removal of thiophenol and diphenyl disulfide are disclosed that make use of functionalized polymers. RO=testosteryl.
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Jaunzems et al. (2003) studied this question.
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