Unsupported and silica-supported H3PMo12O40 catalysts show a wide temperature range for decomposition on thermal treatment allowing the formation of monoclinic β-MoO3(characterized by Raman spectroscopy and X-ray powder diffraction); this new supported phase leads specifically to dimethoxymethane in the methanol oxidation reaction.
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Fournier et al. (1994) studied this question.
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