The complex fluorides LiYF 4 , KYF 4 , BaBeF 4 and AYF 4 Eu x (A = Li, K) are hydrothermally synthesized at 140–240 °C and characterized by powder X-ray diffraction, thermogravimetric analysis, IR spectroscopy, scanning electron microscopy and luminescence measurements.
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Zhao et al. (1997) studied this question.