Two novel and convenient methods for obtaining volatile mercury and methylmercury species for analysis that allows non-volatile analyte solutions to be identified by element-specific and species-selective techniques are described. Non-volatile aqueous solutions of mercury(II) and/or methylmercury(II) compounds are converted into volatile forms (including hydrides) using NaBH4 or LiB(C2H5)3H, followed by chromatographic separation. The volatile derivatives separated on a column are detected by atomic absorption spectrometry or mass spectrometry.
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Craig et al. (1992) studied this question.
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