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Silver, bismuth, and bismuth-silver nanoparticles were synthesized and characterized by cyclic voltammetry, electrochemical impedance spectroscopy, ultraviolet-visible spectroscopy, infrared spectroscopy, Raman spectroscopy, and transmission electron microscopy to determine the electrochemical, optical, structural, and morphological properties of the nanomaterials. The silver, bismuth, and bismuth-silver nanoparticles were shown to have an average particle size of 10–30 nanometers by microscopy. The electrochemical results showed that the bismuth-silver nanoparticles exhibited good electrocatalytic activity that can be harnessed for sensor construction and related applications. The ultraviolet-visible, infrared, and Raman spectroscopy results confirmed the structural properties of the bismuth-silver nanoparticles. In addition, the microscopy and electron diffraction morphological characterization confirmed the nature of the bismuth-silver nanoparticles.
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Horst et al. (2014) studied this question.
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