A head of the game: A new probe head for simultaneous NMR and UV/Vis spectroscopic measurements is designed. 1H NMR and UV/Vis spectra of an intermolecular hydrogen-bonded complex (see scheme) are measured simultaneously in CD2Cl2 at 175 K. Aided by the 1H NMR spectra, the sample concentration can be adjusted so that the desired complex is the exclusive form of the phenol present. The UV/Vis spectra allow the approximate position of the bridging proton to be found.
No takes yet. Share an insight, caveat, or question.
Tolstoy et al. (2009) studied this question.
Synapse has enriched 5 closely related papers on similar clinical questions. Consider them for comparative context: