A double-layered tetrathiafulvalenophane with four alkylenedithio spacers has been synthesized as a novel electron donor. Its structure has been elucidated by an X-ray crystal analysis to have a pair of face-to-face tetrathiafulvalenes with a small cavity in the center. Its electronic spectrum and cyclic voltammetry show a transannular interaction between both TTF units.
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Matsuo et al. (1995) studied this question.
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