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The composition and the crystal structure of corrosion scales from steel pipes have been analysed. High concentrations of green-rust-type phases have been detected in samples mounted on the axis of diffractometer as suspension in native water. This type of sample loading combined with measurements at the high-resolution powder-diffraction beamline (ID31/ESRF) has proven useful in the phase determination of the studied corrosion products.
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Piszora et al. (2009) studied this question.
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