A new approach to the preparation of boron-containing siloxanes based on cluster boron anions has been suggested. This approach consists in the reaction of hydroxy derivatives of closo-decaborate anion [B10H10–n(OH)n]2– (n = 1, 2) with dihalosilanes SiR2Cl2 (R = CH3, t- C4H9, C6H5). The obtained compounds have been characterized by IR, ESI/MS, and NMR (1H, 11B, 13C) spectroscopy.
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Klyukin et al. (2018) studied this question.
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