The utility of 13C‐NMR spectroscopy in the study of organometallic radicals has been demonstrated for substituted nickelocenes. The shifts and halfwidths, as well as their variation, permit structural elucidation of radicals where ESR fails, and provide indications, e.g. of the number of unpaired electrons and their incorporation in various orbitals, and even of isotope effects.
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Köhler et al. (1980) studied this question.
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