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An X‐ray diffraction microstructural study on 110, 220, 001 and 111 peaks has been performed on mullite in the temperature range of primary mullite formation in order to monitor nucleation and growth process. Considering the crystallinity of the starting kaolinites, a greater disorder of the kaolinite has been found to enhance the mullite formation. Isothermal growth is related to a decrease in the Al2O3 content of mullite.
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Serrano et al. (1996) studied this question.
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