Crystal structure of N , N ′-(4,6-dichloro-1,3-phenylene)bis-(3,5-dichlorosalicylaldiminato)-k 4 N,N′,O,O′ nickel(II) monohydrate, mono-ethylacetate solvate C 24 H 18 Cl 6 N 2 NiO 5 | Synapse
May 10, 2026Zeitschrift für Kristallographie - New Crystal Structures0 citationsOpen Access
Crystal structure of N , N ′-(4,6-dichloro-1,3-phenylene)bis-(3,5-dichlorosalicylaldiminato)-k 4 N,N′,O,O′ nickel(II) monohydrate, mono-ethylacetate solvate C 24 H 18 Cl 6 N 2 NiO 5
To determine the crystal structure of a nickel(II) complex with specific ligands and analyze its geometric parameters.
Utilized X-ray diffraction to characterize the crystal structure of the compound.
Studied the molecular formula C24H18Cl6N2NiO5 at 150 K.
Described the crystallographic details including space group and unit cell dimensions.
Identified monoclinic space group C2/c with unit cell dimensions: a = 22.4392(4) Å, b = 17.4135(3) Å, c = 15.3474(3) Å.
Measured the angle β = 118.248(1)°, contributing to the understanding of molecular geometry.
Calculated the volume of the unit cell as V = 5282.73(17) Å3.
Abstract
Abstract C 24 H 18 Cl 6 N 2 NiO 5 (M = 685.81 g/mol): monoclinic, space group C 2/ c (no. 15), a = 22.4392(4) Å, b = 17.4135(3) Å, c = 15.3474(3) Å, β = 118.248(1)°, V = 5282.73(17) Å 3 , Z = 8, T = 150 K.