Scaling up mechanochemical reactions: linking crystalline phase evolution studied via in situ PXRD with kinetics from MCR-ALS

Key Points

• The research aims to connect crystalline phase evolution with kinetic models to improve mechanochemical reaction scalability.
• Utilized an in situ PXRD platform for real-time observation of phase changes.
• Applied MCR-ALS for kinetic modeling of the mechanochemical processes.
• Analyzed the evolution of crystalline phases during mechanochemical reactions.
• Identified specific phase evolution patterns correlating with reaction kinetics.
• Developed reliable kinetic models that support scalable mechanochemical processes.