Electrochemical synthesis creates 4-sulfenylisocoumarins with thiophenols, suggesting safer reactions and broader substrate scope.
Abstract The first example of directly using abundant, stable, and inexpensive thiophenols as sulfenylating agents for the construction of valuable and structually diverse 4-sulfenylisocoumarins under electrochemical conditions is described. Compared to the existing methods, this approach avoids the use of toxic, moisture-sensitive, pre-functionalized reagents and significantly broadens the substrate scope.
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Ma et al. (2025) studied this question.
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