Investigation of Pressure Vacuum Impregnation Using Inorganic, Organic, and Natural Fire Retardants on Beech Wood (Fagus sylvatica) and Its Impact on Fire Resistance

This article investigates the effects of pressure vacuum impregnation using inorganic, organic, and natural flame retardants on enhancing the fire resistance and chemical composition of structural beech wood (Fagus sylvatica). The study examines fire resistance characteristics such as the limiting oxidation number and heat of combustion, which indicate the effectiveness of the flame retardants used. Chemical changes in the beech wood were characterized through various analyses, including changes in chemical composition, FTIR spectra, DSC thermograms, and SEM images. The relationships between combustion characteristics and chemical changes were assessed using multiple methods. The results demonstrate that using 5% potassium acetate achieved a lower heat of combustion compared to 15% sodium phosphate, and it was significantly lower than the heat of combustion observed with 5% arabinogalactan or the reference sample of beech wood. However, neither potassium acetate nor diammonium phosphate significantly affected the macromolecular structures of the wood when compared to the reference sample. Low concentrations of flame retardants reduce environmental release and environmental impact while increasing fire resistance, which could be used for structural solutions made of hardwoods.