This review explores automated electrochemical platforms improving reaction preparation and analysis, highlighting self-driving laboratories.
Automated electrochemical platforms are attracting attention for their potential in streamlining reaction preparation, electrolysis, and analysis to generate large datasets in a fast and efficient manner. Moreover, the recent implementation of on‐line analytics together with closed‐loop workflows has enabled the emergence of electrochemical self‐driving laboratories. In this review, the common guidelines for the development of these platforms are presented, covering the main modules to assemble these systems. Furthermore, a comprehensive survey of all the platforms applied in synthetic organic electrochemistry is reported, where each example is described in terms of elements and applications and classified by category. Finally, an outlook including a perspective on the topic is presented, proposing potential future directions of the field.
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Rial‐Rodríguez et al. (2025) studied this question.
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