Experimental analysis reveals how grain size and long-period stacking-ordered phases affect hot deformation behavior.
The hot deformation behavior of a Mg-9.2Er-4.9Sm-2.2Zn-0.6Zr (wt.%) alloy, with emphasis on the role of grain size and long-period stacking-ordered (LPSO) phases, was examined via comparison experiments. Two types of samples were obtained through distinct heat treatment schedules: sample A had a smaller grain size, featuring block-shaped LPSO phases at grain boundaries and lamellar LPSO phases within grains, while sample B had a larger grain size and few LPSO phases. The hot deformation behavior was characterized by the true stress–strain curve within the processing window of 300–450 °C and 0.001–1 s−1. The block-shaped LPSO phases contributed more significantly to strain hardening, leading to elevated flow stress in sample A, particularly under low-temperature and high-strain-rate conditions. Through the particle-stimulated nucleation (PSN) mechanism, block-shaped LPSO phases demonstrated greater efficiency in promoting Dynamic recrystallization (DRX) compared to lamellar LPSO phases; additionally, the synergistic effect between LPSO phases and grain boundary density further improved DRX efficiency. During hot deformation, dynamic precipitation of both block-shaped and lamellar LPSO phases occurred. The formation of block-shaped phases required a longer duration than that of lamellar ones. The presence of the LPSO kink exerted an influence on DRX, while a significant angle kink can promote DRX.
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Shao et al. (2025) studied this question.
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