We developed a thermomechanical devulcanization process of ground tire rubber (GTR) by incorporating chemicals to achieve better devulcanization. The samples were devulcanized in a twin-screw extruder with the help of three types of chemicals that aid devulcanization: N-(cyclohexylthio) phthalimide (PVI), dibenzamid diphenyl disulfide (DBD) and dialkyl-pentasulfide (DPS, commercialized as Aktiplast 79). We characterized the resulting devulcanizates by Soxhlet-extraction, and produced vulcanized sheets, which we characterized mechanically and examined the vulcanization process. We found that all chemicals facilitated better devulcanization and the devulcanizate had a more rubber-like behavior during mixing. Vulcanization was also slightly improved and reversion was reduced. When revulcanized, the rubber had improved strain at break and tear strength.
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Görbe et al. (2024) studied this question.
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