1,3-Enynes are valuable coupling partners in transition-metal-catalyzed C-H functionalizations. Certainly, aliphatic-substituted 1,3-enynes have been thoroughly investigated in C-H functionalizations, whereas aromatic-substituted 1,3-enynes remain underexplored. Herein, we report the realization of this goal, where we achieve an atom-economical protocol for the synthesis of γ-spirolactams via Rh(III)-catalyzed C-H functionalization of
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Kumar et al. (2024) studied this question.
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