Hydroclimate variation and vegetation changes of the Nile River watershed area in northeast Africa since the Last Glacial Maximum (LGM) were reconstructed based on n‐alkanes, their carbon isotope ratios (δ 13 C n‐alkanes ), and their hydrogen isotope ratios (δ 2 H n‐alkanes ) in sediments from ODP Site 967 in the Eastern Mediterranean Sea. The results were compared with the present vegetation cover in the watershed areas using ArcGIS. The average proportion of current grassland in the Equatorial Lake and Ethiopian Highland Plateaus watershed areas was 45.8 and 64.7%, respectively. δ 2 H n‐alkanes ranged from −199 to −127‰ and co‐varied with insolation change response to orbital forcing. Depleted δ 2 H n‐alkanes were found from deglaciation to the middle Holocene, suggesting increased precipitation during the African Humid Period (AHP) from 15 to 5 ka caused by northward migration of the Intertropical Convergence Zone. However, lower precipitation was inferred by enriched δ 2 H n‐alkanes during the LGM and late Holocene. δ 13 C n‐alkanes at Site 967 did not show a trend in harmony with δ 2 H n‐alkanes and instead exhibited millennial‐scale variations ranging from –25.9 to –33.2‰. These δ 13 C n‐alkanes values consistently indicated a C4 grass‐dominated environment in the watershed areas of the River Nile since the LGM, persisting through the AHP and into the present. Reconstructions demonstrated orbital and abrupt forcing of hydroclimate variability while maintaining generally grass‐dominated vegetation with weak precipitation feedback over the late Quaternary.
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