This work studies the effect of the substrate temperature on the microstructure and properties of CoCrFeNiNb x high entropy alloy (HEA) coatings fabricated by magnetron sputtering. The results indicate that all three CoCrFeNiNb x HEA coatings were composed of a simple FCC solid solution with a columnar structure. As the substrate temperature increased, Nb content in the FCC matrix increased while the grain size first decreased and then increased. Accordingly, CoCrFeNiNb x HEA coatings exhibited an increasing micro-hardness and a decreasing fracture toughness with the increasing substrate temperature. Moreover, CoCrFeNiNb x HEA coating deposited at 200 ∘ had better corrosion performance, which was due to its better surface quality and denser columnar structure compared to the other two coatings.
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Hao et al. (2024) studied this question.
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