Experimental analysis reveals exfoliation efficiency varies with ion implantation order, suggesting new methods.
The physical mechanisms of surface morphology and internal defect evolution of samples implanted with H and He ions in different orders (H-alone, H first then He and He first then H) were systematically investigated by using various methods such as optical microscopy and transmission electron microscopy. However, with the increase of annealing temperature, the He-first sample had higher film exfoliation efficiency compared to the other two groups. The exfoliation of a large-area Ge thin film with a thickness of 656.4 nm had been achieved. In addition, the dynamic process of bubble and defect evolution inside samples co-implanted with H and He ions was analyzed at different annealing temperature stages. Finally, A physical model for surface blistering of Ge wafers implanted with H and He ions was established based on ion damage physics, gas diffusion dynamics, and thin film mechanics theory, which can provide quantitative prediction tools for the smart-cut process of Ge wafers.
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Li et al. (2025) studied this question.
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