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This is a Experimental Study study.

October 23, 2025Angewandte ChemieOpen Access

Stereoselective Synthesis of Alkenyl Fluorides and Alkynes by Defluoro Coupling of Trifluoromethyl Arenes

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Stereoselective synthesis achieves over 98:2 selectivity in alkynes from trifluoromethyl arenes.
Products yielded up to 94% from C–C coupling using functional organodiboron reagents.
Assessment using defluoro coupling method produces diverse products with practical applications.
This method supports efficient construction of complex molecules, enabling multiple transformations.

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Observational analysis shows high selectivity in alkynes, highlighting the utility of aryl trifluoromethyl groups.

Rosario‐Collazo et al. (2025) studied this question.

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