Electrochemical process yields amine derivatives from triethylamines and isocyanonaphthalenes, suggesting new synthetic routes.
A direct electrochemical oxidative cascade cyclization of 2-isocyanonaphthalenes with triethylamines, employing elemental selenium or sulfur, has been developed for the synthesis of 2-aminonaphthoselenazole and 2-aminonaphthothiazole derivatives. A diverse array of aliphatic and aromatic tertiary amines served as the amine source through a C-N bond selective cleavage pathway under metal catalyst-free and external chemical oxidant-free conditions.
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Wu et al. (2025) studied this question.
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