Experimental setup improves synchrotron X-ray diffraction in magnetic fields, indicating enhanced research on crystals.
A specialized experimental setup has been designed and manufactured for X-ray diffraction studies under the influence of external magnetic fields on the sample. The setup includes a set of precision automated electromechanical drives that enable orientation of the permanent magnet-based magnetic system along various crystallographic directions of the studied sample. The system provides automated variation of the external magnetic field strength and direction during the experiment. The setup is compatible with blow-out type temperature attachments, allowing for research within a wide temperature range. The specified performance characteristics of the setup and its high parameter stability have been validated through a series of experiments with X-ray scattering near absorption edges using iron borate single crystals.
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N. I. Snegirev (2025) studied this question.
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