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January 6, 2026CrystEngComm0 citations

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A dynamic pcu MOF(Zn) containing a ditopic T-shaped 2rotaxane linker

HAHazem AmarneUniversity of Jordan ASAlexander J. StirkUniversity of Windsor COChristopher A. O’KeefeUniversity of Windsor

Key Points

To investigate the structural properties of a pcu MOF utilizing a T-shaped [2]rotaxane linker.
Synthesis of a pcu MOF designated UWDM-16 using a ditopic T-shaped [2]rotaxane linker
Single crystal X-ray diffraction (SCXRD) to analyze pore occupancy
Solid-state NMR spectroscopy (2H SSNMR) to assess the mobility of the macrocyclic wheel
Rotaxanes were confirmed to occupy the pores within the material
Solid-state NMR revealed the macrocyclic wheel's mobility in the MOF structure

Abstract

A T-shaped 2rotaxane linker was used to make a pcu MOF, designated UWDM-16 . SCXRD showed the rotaxanes occupy pores in the material and 2 H SSNMR verified that the macrocyclic wheel is mobile in the solid-state.

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A dynamic pcu MOF(Zn) containing a ditopic T-shaped 2rotaxane linker | Synapse

Cite This Study

Amarne et al. (Thu,) studied this question.

synapsesocial.com/papers/695d85413483e917927a44f2 https://doi.org/https://doi.org/10.1039/d5ce01108f