We investigate the mechanical properties of electrospun boron nitride nanotube (BNNT)-reinforced silica nanocomposite microfibers. The incorporation of small amounts of BNNTs (0.1, 0.3, and 0.5 wt.%) into silica results in significant enhancements in the bulk mechanical performance, including up to a 26.4% increase in Young’s modulus, a 19.4% increase in tensile strength, and a 12.8% increase in toughness. These improvements are attributed to the excellent nanotube alignment achieved via electrospinning and the effective transfer of interfacial loads at the BNNT–silica interface. Micromechanical analysis based on in situ Raman measurements reveals that the maximum interfacial shear stress in the electrospun BNNT–silica microfiber reaches about 341 MPa. This study provides new insights into the process–structure–property relationship and reinforcement mechanisms in nanotube-reinforced ceramic nanocomposites, thereby advancing the development of lightweight, strong, tough, and durable ceramic materials.
Wang et al. (Sat,) studied this question.