Thermoelectrochemistry-enabled phase and morphology control of metal phosphide nanocrystals

Key Points

• This research aims to enhance the control over nanocrystal morphology in the synthesis of metal phosphides using thermoelectrochemistry.
• Utilized thermoelectrochemistry for direct synthesis of transition metal phosphides.
• Implemented selective surface heating during the electrochemical synthesis process.
• Analyzed the resulting morphology and phase of the generated nanocrystals.
• Achieved precise control over nanocrystal morphology without extensive thermal treatment.
• Demonstrated that selective surface heating effectively modifies the phase of metal phosphide nanocrystals.