Novel synthesis demonstrates high yields of thiocoumarin derivatives, highlighting significant synthetic utility.
A [4+2] annulation reaction between 1,2,3‐thiadiazoles and para ‐quinone methides has been achieved. Various functionalized thiocoumarins are successfully obtained in up to 96% yield. The synthetic utility of this protocol is demonstrated by the 30 mmol scale reaction.
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Zhu et al. (2026) studied this question.
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