Hydrothermal synthesis and crystal structure of poly{tris(μ ₂ - cis -1,4–cyclohexanedicarboxylato)-κ ² O: O ′ ] -bis[μ ₃ -1,3,5-tris[(1 H -imidazol-1-yl)methyl]benzene-κ ³ N, N ′ ,N ″ ]trizinc(II)} trihydrate, C ₆₀ H ₇₂ N ₁₂ O ₁₅ Zn ₃

D.Q. Jiang; Yue Zhou; Kai-Long Zhong

doi:10.1515/ncrs-2025-0479

February 13, 2026Zeitschrift für Kristallographie - New Crystal StructuresOpen Access

Hydrothermal synthesis and crystal structure of poly{tris(μ ₂ - cis -1,4–cyclohexanedicarboxylato)-κ ² O: O ′ ] -bis[μ ₃ -1,3,5-tris[(1 H -imidazol-1-yl)methyl]benzene-κ ³ N, N ′ ,N ″ ]trizinc(II)} trihydrate, C ₆₀ H ₇₂ N ₁₂ O ₁₅ Zn ₃

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Key Points

The study aims to characterize the crystal structure of a tris-zinc complex synthesized using hydrothermal methods.
Synthesis of poly{tris(μ2-cis-1,4–cyclohexanedicarboxylato)-κ2O:O′]-bis[μ3-1,3,5-tris[(1H-imidazol-1-yl)methyl]benzene-κ3N,N′,N″]trizinc(II) in hydrothermal conditions.
X-ray diffraction analysis performed to determine crystal structure and parameters.
Characterization of the compound at a temperature of 293 K.
The compound crystallizes in a trigonal structure with R32 symmetry.
Unit cell dimensions were found to be a = 17.9308(7) Å and c = 36.533(2) Å.
Calculated volume of the crystal is 10172.2(10) Å3.

Implication

Research demonstrates the crystal structure of a zinc complex synthesized hydrothermally, revealing its unique properties.

Abstract

C 60 H 72 N 12 O 15 Zn 3 , trigonal, R 32 (no. 155), a = 17.9308(7) Å, c = 36.533(2) Å, V = 10172.2(10) Å 3 , Z = 18, R gt ( F ) = 0.0533, w R ref ( F 2 ) = 0.1488, T = 293 K.

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Cite This Study

Jiang et al. (2026) studied this question.

synapsesocial.com/papers/6996a82decb39a600b3eea71 https://doi.org/10.1515/ncrs-2025-0479

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Hydrothermal synthesis and crystal structure of poly{tris(μ ₂ - cis -1,4–cyclohexanedicarboxylato)-κ ² O: O ′ ] -bis[μ ₃ -1,3,5-tris[(1 H -imidazol-1-yl)methyl]benzene-κ ³ N, N ′ ,N ″ ]trizinc(II)} trihydrate, C ₆₀ H ₇₂ N ₁₂ O ₁₅ Zn ₃

Key Points

Implication

Abstract

Discussion

Cite This Study

Hydrothermal synthesis and crystal structure of poly{tris(μ ₂ - cis -1,4–cyclohexanedicarboxylato)-κ ² O: O ′ ] -bis[μ ₃ -1,3,5-tris[(1 H -imidazol-1-yl)methyl]benzene-κ ³ N, N ′ ,N ″ ]trizinc(II)} trihydrate, C ₆₀ H ₇₂ N ₁₂ O ₁₅ Zn ₃

Key Points

Implication

Abstract

Discussion

Cite This Study

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