Photocatalytic transformation generates thioester oximes from alkenes, suggesting a sustainable synthesis method.
A visible-light-induced oximo-thioesterification of alkenes with tert-butyl nitrite and thioacids leading to the formation of α-thioester oximes has been developed. This transformation provides a series of diverse α-thioester oximes in moderate to good yields at room temperature. The present photocatalytic protocol has the advantages of metal-free condition, simple operation, green energy source, and favorable functional group tolerance.
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Yang et al. (2026) studied this question.
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