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This experiment demonstrates the oxidation of piperonyl alcohol to piperonal using IBX in organic chemistry students, highlighting its simplicity and effectiveness.
This manuscript describes an experiment suitable for sophomore or advanced organic chemistry students involving the oxidation of piperonyl alcohol to piperonal using the hypervalent iodine oxidizing agent IBX (o-iodoxybenzoic acid). The reaction is simple to carry out in one lab period, and gives the product in good yield and purity without purification.
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More et al. (2017) studied this question.
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