Experimental study demonstrates accelerated synthesis of UiO-66 and UiO-67 frameworks using hydrochloric acid, indicating an efficient pathway to highly porous materials.
A scalable, reproducible method of synthesizing UiO-66- and UiO-67-type MOFs, entailing the addition of HCl to the reaction mixture, has been investigated. The new protocol requires a fraction of the time of previously reported procedures, yields exceptional porosities, and works with a range of linkers.
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Katz et al. (2013) studied this question.
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