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April 10, 2026Organic LettersOpen Access

Enantioselective Rh/Cu-Catalyzed Addition of Terminal Alkynes to Allenes for the Synthesis of Chiral 1,4-Enynes

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Authors

MDMartin T. DaigerJKJanika KromerSKSamuel Kaplan

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Overview

This report demonstrates a novel method for synthesizing chiral 1,4-enynes using rhodium/copper catalysis, highlighting its broad functional-group tolerance.

Key Points

  • To develop a regio- and enantioselective catalytic method for synthesizing chiral 1,4-enynes from terminal alkynes and allenes.
  • Utilized rhodium/copper catalyst for the coupling reaction.
  • Employed terminal alkynes and allenes as starting materials.
  • Assessed the reaction yields and enantioselectivities.
  • Evaluated functional-group tolerance of the resulting products.
  • Achieved high yields in the synthesis of chiral 1,4-enynes.
  • Demonstrated excellent enantioselectivities in the reaction.
  • Showcased broad functional-group tolerance in the coupling process.

Cite This Study

Daiger et al. (2026) studied this question.

synapsesocial.com/papers/69d8940c6c1944d70ce0510ahttps://doi.org/10.1021/acs.orglett.6c01096
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