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Mechanosynthesis produces α-bromoacrylates in a one-pot process, suggesting efficient chemical reactions without solvents.
A mechanosynthesis of α-bromoacrylates was described from commercially available triethyl phosphonoacetate by using a ball-milling-assisted bromination/HWE one-pot process. Initially, the bromination and the HWE protocols were independently optimized under mechanochemical...
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Caldiero et al. (2026) studied this question.
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