The method finds oxidative coupling of thiocarboxylic acids and amines improves peptide bond formation, indicating a mild strategy.
We report a mild and epimerization-free strategy for peptide bond formation based on a TEMPO-promoted oxidative coupling of thiocarboxylic acids with amines. In this protocol, thiocarboxylic acids are selectively oxidized...
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Singh et al. (2026) studied this question.
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