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Getting down to business: Reduction of the LaIII tricyclopentadienide complex LaCp′′3 (Cp′′=η5-1, 3- (SiMe3) 2C5H3) by K and 18crown-6 or 2, 2, 2cryptand produced thermally stable mononuclear crystalline lanthanate (II) salts. The La +2 oxidation state in these complexes was confirmed both in solution (EPR) and the solid state (EPR, SQUID, X-ray diffraction) and was supported by a computational study. Supporting information for this article is available on the WWW under http: //www. wiley-vch. de/contents/jc₂002/2008/z704887ₛ. pdf or from the author. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article.
Hitchcock et al. (Fri,) studied this question.
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