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May 17, 2026Food Chemistry0 citationsOpen Access

Fully portable smartphone-integrated device coupled with nanozyme-based assay for sensitive detection of TBHQ in edible oils.

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QWQianyi WuMFMarcus Vinicius da Silva FerreiraMKMohammed Kamruzzaman

Key Points

  • The aim is to develop a portable device for sensitive detection of TBHQ in edible oils using a nanozyme-based assay.
  • Synthesis of an organic peroxidase-like nanozyme through self-assembly.
  • Development of a 3D-printed platform integrated with a smartphone app for real-time detection.
  • Conducted colorimetric assays to quantify TBHQ levels in commercial oils.
  • Achieved a limit of detection about 330,000-fold below permitted TBHQ levels in foods.
  • Demonstrated high recovery rates for TBHQ detection in peanut and soybean oils.
  • Showed strong analytical performance indicating accuracy and robustness for on-site monitoring.

Abstract

Tert-butylhydroquinone (TBHQ) is a synthetic antioxidant widely used in edible oils to extend shelf life, yet excessive intake has been linked to potential carcinogenic risks, underscoring the need for reliable routine monitoring. However, conventional analytical techniques for detecting TBHQ are often costly, complex, and impractical for rapid on-site screening. In this study, a fully organic nanozyme (TPNZ) was synthesized via self-assembly and employed as a peroxidase-mimetic catalyst for the colorimetric quantification of TBHQ. To enable field-deployable analysis, a portable 3D-printed detection platform was further developed and integrated with a custom smartphone application capable of real-time RGB and ΔE colorimetric evaluation. Notably, this portable system achieved a limit of detection (LOD) approximately 330,000-fold below the maximum permitted TBHQ concentration in food products. Furthermore, the system achieved high recovery rates for TBHQ detection in commercial peanut and soybean oil samples, demonstrating its accuracy, robustness, and potential practical applicability for on-site TBHQ monitoring. • Synthesis of fully organic peroxidase-like nanozyme through simple self-assembly. • Nanozyme-based colorimetric assays for sensitive TBHQ detection. • Integration of a 3D-printed platform and a mobile app for real-time color analysis. • Strong analytical performance for TBHQ monitoring in commercial edible oils.

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Cite This Study

Wu et al. (2026) studied this question.

synapsesocial.com/papers/6a095c3f7880e6d24efe24a7https://doi.org/10.1016/j.foodchem.2026.149610
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