Crystallographic analysis demonstrates room-temperature crystallization of [Pd6Cl12] clusters in thionyl chloride, indicating that reducing carbon monoxide pressure enables facile crystal growth.
A reduction of the CO partial pressure is sufficient to obtain single crystals of [Pd 6 Cl 12 ] from the equilibrium (a) in thionyl chloride (solv.) at room temperature. The single‐crystal and powder X‐ray diffraction characterization of this Pd II chloride is described. equation image
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Dell’Amico et al. (1996) studied this question.
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