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The insect moulting hormone crustecdysone has been isolated from the Australian brown pine, Podocarpus elatus R.Br., and detected in a number of other Podocarpus species from various parts of the world. A series of acetates and acetonides of crustecdysone has been prepared, and the mass and nuclear magnetic resonance spectra of these compounds analysed. A simple micro method of measuring the rate of acetylation of hydroxy groups in steroids has been developed to determine the steric environment of these groups.
Galbraith et al. (Thu,) studied this question.