Syntheses and Properties of Pentafluoroethylplumbanes in the Oxidation States +II, +III, and +IV

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This research aims to synthesize and characterize pentafluoroethylplumbanes in various oxidation states. It explores different aryl substituents and their effects on synthesis.
Synthesized mono-, bis-, and tris(pentafluoroethyl)plumbanes by treating arylchloroplumbanes with LiC2F5.
Used HCl for further treatment to create chloro(pentafluoroethyl)plumbanes.
Characterized compounds through multinuclear NMR spectroscopy and single crystal x-ray diffraction.
Successfully synthesized and characterized a range of pentafluoroethylplumbanes, including the tris(pentafluoroethyl)plumbate(II) anion.
Formation of Pb(C2F5)4 achieved from Pb(OAc)4, fully characterized using advanced techniques.
The synthesis showed potential for versatile applications in various oxidation states.

Investigates the synthesis and properties of pentafluoroethylplumbanes, highlighting their diverse oxidation states.

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Grasse et al. (2026) studied this question.

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