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The kinetics of the copolymerization of N ‐isopropylacrylamide (NiPAAm) and diethylene glycol monomethylether monomethacrylate was followed by online 1 H NMR spectroscopy. Two copolymerization reactions were sufficient to evaluate the kinetic data with the Extended‐Kelen–Tüdös method as well as the nonlinear least square method. The copolymerization parameter was determined as r NiPAAm = 0.70 and r DEGMA = 2.0. The higher reactivity of the methacrylate compared to the NiPAAm is in good agreement with other kinetic data of similar systems.
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Gramm et al. (2004) studied this question.
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